ASTM a Test, Intergranular Corrosion, IGC, ASTM A Practice, Testing, India – Download as PDF File .pdf), Text File .txt) or read online. ASTM A Practice A test (Oxalic acid test). The oxalic acid etch test is rapid and nondestructive, but not quantitative. It is a rapid etching procedure and . Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials practie quantitatively. These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. This method is preferable for chromium depletions and corrosion in intermetallic phases.
Historical Version s – view previous versions of standard Work Item s – proposed revisions of this standard Translated Version s: Wilson Hardness Conversion Chart. Due to the variance of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion.
Contact us now for pricing or a quote! Please refer to the specification for more details. The samples are etched after metallographic practtice for cross-sectional examination which is thoroughly viewed with a traverse from inside to outside diameters of rods and tubes, from face to face on plates, and across all zones such as weld metal, weld-affected zones, and base plates on specimens containing welds.
Intergranular corrosion shows up as the dark black lines around the grain boundaries. Historical Version s – view previous versions of standard.
If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed.
It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.
This abstract is a brief summary of the referenced standard. The test evaluates the resistance of extra-low-carbon steels to sensitization and intergranular attack from welding or heat treatment processes. The chart below comes from the ASTM A standard for selection of the appropriate test by alloy type:.
The samples are weighed at each interval to determine mass loss and degree of susceptibility aastm intergranular attack. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice. Work Item s – proposed revisions of this standard.
All austenitic stainless steels should meet this requirement, if proper annealing took place. What is your typical turnaround time?
The test uses a visual inspection of the surface of the bent specimen to determine pass or fail.
ASTM A Intergranular Corrosion Testing and Analysis
Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. 2a62 recent publication on intergranular corrosion. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated.
The inch-pound equivalents are in parentheses and may be approximate. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on. All five methods within this specification involve exposing specimens praxtice a chemical mixture designed to encourage corrosive behavior. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid.
To understand intergranular corrosion testing or intergranular attack commonly abbreviated as IGC or IGAit is important to understand what causes the process to occur. Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to pratcice intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.
Link to Asrm This link will always route to the current Active version of the standard. Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack.
Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack for low carbon steels. In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results.
If the structure is acceptable no additional testing is required. It depends on which Practice is selected, but typically ranges from to days for different tests. If you are not sure, please contact us for assistance. Like what you saw?
Intergranular Corrosion Testing: An Overview of ASTM A262
Metals like stainless steels and aluminum contain elements such as niobium and chromium, often integrated because of their natural corrosion resistance. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys. Practice A is a rapid screening examination of the microstructure to quickly determine if the structure is certain to be free of susceptibility to rapid intergranular attack. Intergranular corrosion is the proper use, though the specification calls it attack, corrosion is what is taking place.
Based on your materials, application, and requirements, the other 4 methods provide specific focuses. This method is a hour boiling test for “as received” specimens of stainless steel.
Learn more about our laboratories – where they are located; the unique capabilities they have and how they can help you solve your technical and commercial challenges. How do you select the right ASTM corrosion testing method for your material? For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. Carbon and Sulfur Analysis. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.
G2MT Labs is one of the few labs to offer all five ASTM A corrosion testing practices, as well as the expertise to help you determine which tests to use, what to do if a test fails, and other corrosion consulting as needed. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.
At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type. The Oxalic Acid test is only used to ensure that no corrosion exists; samples are labeled either “Acceptable” or “Suspect”.
From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment.